This article describes a collaborative project between researchers in the Mathematics and Computer Science Division at Argonne National Laboratory and the Computer Music Project of the University of Illinois at Urbana-Champaign. The project focuses on the use of sound for the exploration and analysis of complex data sets in scientific computing. The article addresses digital sound synthesis in the context of DIASS (Digital Instrument for Additive Sound Synthesis) and sound visualization in a virtual-reality environment by means of M4CAVE. It describes the procedures and preliminary results of some experiments in scientific sonification and sound visualization.